Voltametria de pulso diferencial (vpd) em estado sólido de manchas de cromatografia de camada delgada (ccd): um novo método de análise para fitoativos antioxidantes

Resumo

A new electroanalytical method coupling TLCDPV in solid state was developed for quantitative determination of phytoantioxidants with medicinal purpose, e.g. rosmarinic acid (RA) in samples of phytopharmaceuticals, e.g. rosemary (Rosmarinus officinalis L.). The method showed to be feasible, presenting linearity in concentrations ranging from 0.694 x 10-3 to 9.526 x 10-3 mol L-1 (r = 0.9945), good sensibility, selectivity, reproducibility, repeatability, agility and affordable cost. The concentrations of RA in different extracts of rosemary ranged from 0.05 to 0.52 (% w/w), presenting high recovery levels when compared to HPLC.

Descrição

Palavras-chave

Chemically modified electrodes, TLC-DPV, Rosmarinic acid

Citação

GONCALVES, Darlene et al. Voltametria de pulso diferencial (vpd) em estado sólido de manchas de cromatografia de camada delgada (ccd): um novo método de análise para fitoativos antioxidantes. Química Nova, São Paulo, v. 34, n. 2, p. 330-334, 2011.