In vivo and in vitro volatile constituents of the flowers of Xylopia aromatica by HS-SPME/GC-MS

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dc.creatorJunqueira, João Gabriel Moraes
dc.creatorNascimento, Michelle Nauara Gomes do
dc.creatorCosta, Lucas Gustavo da
dc.creatorRomualdo, Lincoln Lucilio
dc.creatorAquino, Francisco Wendel Batista de
dc.creatorAbubakar, Mustapha N.
dc.creatorTerezan, Ana Paula
dc.creatorCunha, Gustavo Odeone da Silva
dc.creatorSeverino, Vanessa Gisele Pasqualotto
dc.date.accessioned2024-11-11T16:40:09Z
dc.date.available2024-11-11T16:40:09Z
dc.date.issued2021-05
dc.description.abstractXylopia aromatica (Lam.) Mart. (Annonaceae) is a typical species from the Brazilian cerrado that presents medicinal properties. The plant is distinguished by its large white flowers which produce a pleasant fragrance. X. aromatica is characterized by a wide range of medicinal application. These characteristics have motivated us to investigate the flowers volatile organic compounds (VOCs) via in vivo and in vitro protocols by a headspace solid-phase microextraction (HS-SPME) technique combined with gas chromatography-mass spectrometry (HS-SPME/GC-MS). Four different fibers, extraction times and temperatures were the parameters changed to lead to the maximum profiling of the volatile constituents. Data were analyzed using principal component analysis (PCA). A total of 77 VOCs were extracted from the floral scent, with 52 and 68 extracted from in vivo and in vitro sampling, respectively, of which 48 were reported for the first time in the literature as volatile constituents from X. aromatica flowers. The extraction and identification of VOCs were successfully performed through HS-SPME/GC-MS. The PCA data allowed the identification of parameters that led to the maximum number of VOCs, which were polyacrylate (PA) and carboxen/polydimethylsiloxane (CAR/PDMS) fibers, 60 min extraction time and temperature of 29.0 °C. Among the volatile constituents identified, sesquiterpenes predominated, comprising about 61.04%.
dc.identifier.citationJUNQUEIRA, João G. M. et al. In vivo and in vitro volatile constituents of the flowers of Xylopia aromatica by HS-SPME/GC-MS. Journal of the Brazilian Chemical Society, São Paulo, v. 32, p. 1111-1119, 2021. DOI: 10.21577/0103-5053.20210013. Disponível em: https://www.scielo.br/j/jbchs/a/rNzH9MBN8nVS669HDbypjyh/abstract/?lang=en. Acesso em: 14 ago. 2024.
dc.identifier.doi10.21577/0103-5053.20210013
dc.identifier.issn0103-5053
dc.identifier.issne- 1678-4790
dc.identifier.urihttp://repositorio.bc.ufg.br//handle/ri/25867
dc.language.isoeng
dc.publisher.countryBrasil
dc.publisher.departmentInstituto de Química - IQ (RMG)
dc.rightsAcesso Aberto
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/4.0/
dc.subjectXylopia aromatica
dc.subjectIn vivo and in vitro sampling
dc.subjectHS-SPME/GC-MS
dc.subjectVOCs
dc.subjectMultivariate analysis
dc.titleIn vivo and in vitro volatile constituents of the flowers of Xylopia aromatica by HS-SPME/GC-MS
dc.typeArtigo

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